Author Topic: Soft emulsion  (Read 969 times)

Nigel

  • Self-Coat
  • *****
  • Posts: 1,523
    • nigel rumsey photography
Soft emulsion
« on: December 17, 2023, 03:02:52 PM »
Hi all,

I developed a couple of rolls of Tri-X this morning, and for the first time that I can remember, I noticed that the emulsion was a little soft. I squeegeed the film as I always do and there was a small amount of emulsion suspended in the water that came off. I've been googling and I can't find any suggestion why this might happen.

My process: Bellini ECO 7 mins, Ilford stop, Ilford Rapid Fix 5 mins, wash. The only thing I was slightly concerned about, because we have such hard water I always do a final rinse in some bottled water. Today that water was quite cold. I'm guessing 12-13°C. I don't think I've ever seen reticulation before. Would I notice it before scanning? Could that be the issue?


 
"Imagination is more important than knowledge." Albert Einstein

website

Francois

  • Self-Coat
  • *****
  • Posts: 15,775
Re: Soft emulsion
« Reply #1 on: December 17, 2023, 04:06:05 PM »
It could be reticulation as you're doing things in the right order in order to get it. (it only works when going from warm to cold)
But Tri-X is usually quite robust, so I'm pretty surprised.

A thing that also softens the emulsion is an alkaline bath.

As for seeing it before scanning, check the negs with a magnifying glass, you should see the mottled texture the process would leave.
Francois

Film is the vinyl record of photography.

Nigel

  • Self-Coat
  • *****
  • Posts: 1,523
    • nigel rumsey photography
Re: Soft emulsion
« Reply #2 on: December 17, 2023, 07:53:36 PM »
Thanks Francois. I've been reading a couple of forums where folks have tried to create reticulation deliberately and have had to resort to a significant temperature difference to get the effect, far more than my 8-ish degrees. It happened to both films, so there's something going on but at the moment I have no other ideas.

Unfortunately, my eyes aren't good enough to detect whether there is any reticulation, so I'll have to wait until scanning.
"Imagination is more important than knowledge." Albert Einstein

website

Francois

  • Self-Coat
  • *****
  • Posts: 15,775
Re: Soft emulsion
« Reply #3 on: December 17, 2023, 08:36:25 PM »
If there is a bit of exposed leader left, you might be able to feel it a bit between your fingers... provided you don't have dry skin like I do...
Francois

Film is the vinyl record of photography.

Francois

  • Self-Coat
  • *****
  • Posts: 15,775
Re: Soft emulsion
« Reply #4 on: December 18, 2023, 02:31:38 PM »
I was wondering something last night: how old is the film?
Francois

Film is the vinyl record of photography.

Nigel

  • Self-Coat
  • *****
  • Posts: 1,523
    • nigel rumsey photography
Re: Soft emulsion
« Reply #5 on: December 19, 2023, 07:31:47 AM »
I was wondering something last night: how old is the film?

It’s a good thought, but I think it expired earlier this year.
"Imagination is more important than knowledge." Albert Einstein

website

Francois

  • Self-Coat
  • *****
  • Posts: 15,775
Re: Soft emulsion
« Reply #6 on: December 19, 2023, 02:46:17 PM »
That's fresh for me.
I had something similar happen to me on some HP5 that expired in 1989 and that was in a mystery bulk loader I got at a garage sale....
Could it have been something left in the tank before this roll?
It's either that or maybe a defect on that particular batch, though kodak's quality control is pretty darn good...
Francois

Film is the vinyl record of photography.